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Sodium tert-butoxide

Sodium tert-butoxide (or sodium t-butoxide) is a chemical compound with the formula (CH<sub>3</sub>)<sub>3</sub>CONa (abbr. NaOtBu). It is a strong, non-nucleophilic base. It is flammable and moisture sensitive. It is sometimes written in the chemical literature as sodium t-butoxide. It is similar in reactivity to the more common potassium tert-butoxide.

The compound can be produced by treating tert-butyl alcohol with sodium hydride.

Reactions

One application for sodium tert-butoxide is as a non-nucleophilic base. It has been widely used in the Buchwald–Hartwig amination, as in this typical example:

Sodium tert-butoxide is used to prepare tert-butoxide complexes. For example hexa(tert-butoxy)ditungsten(III) is thus obtained by the salt metathesis reaction from a ditungsten heptachloride:

NaW<sub>2</sub>Cl<sub>7</sub>(THF)<sub>5</sub> + 6 NaOBu-t → W<sub>2</sub>(OBu-t)<sub>6</sub> + 7 NaCl + 5 THF

Structure

Sodium tert-butoxide forms clusters in the solid state, both hexamers and nonamers.

Related compounds

References