my-server
← Wiki

Ruthenium pentacarbonyl

Ruthenium pentacarbonyl is the ruthenium compound with the formula Ru(CO)<sub>5</sub>. It is a colorless, light-sensitive liquid that readily decarbonylates upon standing at room temperature. It is of academic interest as an intermediate for the synthesis of metal carbonyl complexes.

Preparation

Ru(CO)<sub>5</sub> was originally prepared by carbonylation of ruthenium salts in the presence of a reducing agent. A more recent preparation involves photolysis of triruthenium dodecacarbonyl in the presence of carbon monoxide:

Ru<sub>3</sub>(CO)<sub>12</sub> + 3 CO 3 Ru(CO)<sub>5</sub>

It is characterized by two intense ν<sub>CO</sub> bands in the IR spectrum at 2038 and 2003&nbsp;cm<sup>−1</sup> (hexane solution).

Comparisons of M(CO)<sub>5</sub> (M = Fe, Ru, Os)

Whereas Fe(CO)<sub>5</sub> is completely robust at room temperature, samples of Ru(CO)<sub>5</sub> are typically reddish owing to contamination by Ru<sub>3</sub>(CO)<sub>12</sub>. The conversion is rapid in solution. Os(CO)<sub>5</sub> requires heating to 80&nbsp;°C to effect conversion to triosmium dodecacarbonyl.

References