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Osmium pentacarbonyl

Osmium pentacarbonyl is the organoosmium compound with the formula Os(CO)<sub>5</sub>. It is the simplest isolatable carbonyl complex of osmium. Osmium pentacarbonyl is a colorless volatile liquid that is obtained by treating solid triosmium dodecacarbonyl under 200 atmospheres of carbon monoxide at 280-290&nbsp;°C. In contrast, also at 200 atm of CO, solid Ru<sub>3</sub>(CO)<sub>12</sub> converts to Ru(CO)<sub>5</sub> at milder temperature of 160&nbsp;°C.

Reactions

Samples of Os(CO)<sub>5</sub> convert back to the trioosmium cluster upon heating to 80&nbsp;°C. The analogous conversion of Ru(CO)<sub>5</sub> back to Ru<sub>3</sub>(CO)<sub>12</sub> occurs at room temperature. Chlorination of the pentacarbonyl gives a cationic pentacarbonyl complex:

Os(CO)<sub>5</sub> + Cl<sub>2</sub> → [Os(CO)<sub>5</sub>Cl]<sup>+</sup>Cl<sup>−</sup>

Upon UV irradiation, hexane solutions of the pentacarbonyl react with ethylene to give mono-, di-, and trisubstituted derivatives:

Os(CO)<sub>5</sub> + nC<sub>2</sub>H<sub>4</sub> → Os(CO)<sub>5-n</sub>(C<sub>2</sub>H<sub>4</sub>)<sub>n</sub> + nCO (n = 1,2,3)

References