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Vanadium tetrafluoride

Vanadium(IV) fluoride (VF<sub>4</sub>) is an inorganic compound of vanadium and fluorine. It is paramagnetic yellow-brown solid that is very hygroscopic. Unlike the corresponding vanadium tetrachloride, the tetrafluoride is not volatile because it adopts a polymeric structure. It decomposes before melting.

Preparation and reactions

VF<sub>4</sub> can be prepared by treating VCl<sub>4</sub> with HF:

VCl<sub>4</sub> + 4 HF → VF<sub>4</sub> + 4 HCl

It was first prepared in this way.

It decomposes at 325&nbsp;°C, undergoing disproportionation to the tri- and pentafluorides:

2 VF<sub>4</sub> → VF<sub>3</sub> + VF<sub>5</sub>

Structure

The structure of VF<sub>4</sub> is related to that of SnF<sub>4</sub>. Each vanadium centre is octahedral, surrounded by six fluoride ligands. Four of the fluoride centers bridge to adjacent vanadium centres.

References

External links