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Silicon tetraiodide

Silicon tetraiodide is the chemical compound with the formula SiI<sub>4</sub>. It is a tetrahedral molecule with Si-I bond lengths of 2.432(5) Å.

SiI<sub>4</sub> is a precursor to silicon amides of the formula Si(NR<sub>2</sub>)<sub>4</sub> (R = alkyl). It has also been of interest in the manufacture and etching of silicon in microelectronics.

Synthesis and reactions

This compound is produced by treating silicon-copper mixture with iodine:

It reacts quickly with water and moisture in the air.

It can also be made on a large scale by reaction of silicon or silicon carbide with iodine on heating to about 200&nbsp;°C. Of more academic interest is the reaction of silane with iodine vapour at 130 - 150&nbsp;°C, as this produces a series of compounds ranging from iodosilane SiH<sub>3</sub>I to diiodosilane SiH<sub>2</sub>I<sub>2</sub> and triiodosilane SiHI<sub>3</sub> as well. These compounds are colourless liquids at room temperature. The last one can be readily distinguished from the similar carbon compound, iodoform which is a yellow solid at room temperature.

Comparison with other SiX<sub>4</sub> compounds

References

External links