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Osmium hexafluoride

Osmium hexafluoride, also osmium(VI) fluoride, (OsF<sub>6</sub>) is a compound of osmium and fluorine, and one of the seventeen known binary hexafluorides.

Synthesis

Osmium hexafluoride is made by a direct reaction of osmium metal exposed to an excess of elemental fluorine gas at 300&nbsp;°C.

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Description

Osmium hexafluoride is a yellow crystalline solid that melts at 33.4&nbsp;°C and boils at 47.5&nbsp;°C. The solid structure measured at −140&nbsp;°C is orthorhombic space group Pnma. Lattice parameters are a&nbsp;=&nbsp;9.387&nbsp;ÃÂ, b&nbsp;=&nbsp;8.543&nbsp;Å, and c&nbsp;=&nbsp;4.944&nbsp;Å. There are four formula units (in this case, discrete molecules) per unit cell, giving a density of 5.09&nbsp;g·cm<sup>−3</sup>.

The OsF<sub>6</sub> molecule itself (the form important for the liquid or gas phase) has octahedral molecular geometry, which has point group (O<sub>h</sub>). The Os–F bond length is 1.827&nbsp;Å.

Partial hydrolysis of OsF<sub>6</sub> produces OsOF<sub>4</sub>.

References

Further reading

External links