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Dihydroxydisulfane

Dihydroxydisulfane or hypodithionous acid is a reduced sulfur oxyacid with sulfur in a formal oxidation state of +1, but the valence of sulfur is 2. The structural formula is , with all atoms arranged in a chain. It is an isomer of thiosulfurous acid but is lower in energy. Other isomers include HOS(=O)SH, HOS(=S)OH, and HS(=O)<sub>2</sub>SH. Disulfur monoxide, S<sub>2</sub>O, can be considered as the anhydride. Unlike many of these other reduced sulfur acids, dihydroxydisulfane can be formed in a pure state by reacting hydrogen sulfide with sulfur dioxide at −70&nbsp;°C in dichlorodifluoromethane.

H<sub>2</sub>S + SO<sub>2</sub> → H<sub>2</sub>S<sub>2</sub>O<sub>2</sub>

Dihyroxydisulfane may exist in an equilibrium with thiosulfurous acid.

Organic derivatives such as dimethoxydisulfane, diaceto disulfide, and bis(trifluoroaceto) disulfide also exist.

The conjugate bases are called disulfanediolate and hypodithionite .

Properties

Calculations predict that the S−S bond length is 2.013&nbsp;Å, O−S bond length is 1.645&nbsp;Å, H−O bond length is 0.943&nbsp;Å.

Related compounds

Related compounds include the isoelectronic substances hydrogen tetroxide HOOOOH, hydroxotrisulfane HOSSSH, HSOSSH, and tetrasulfane HSSSSH.

References