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Hexanitroethane

Hexanitroethane (HNE) is an organic compound with chemical formula C<sub>2</sub>N<sub>6</sub>O<sub>12</sub> or (O<sub>2</sub>N)<sub>3</sub>C-C(NO<sub>2</sub>)<sub>3</sub>. It is a solid matter with a melting point of 135 °C.

Hexanitroethane is used in some pyrotechnic compositions as a nitrogen-rich oxidizer, e.g. in some decoy flare compositions and some propellants. Like hexanitrobenzene, HNE has been investigated as a gas source for explosively pumped gas dynamic lasers.

A composition of HNE as oxidizer with boron as fuel is being investigated as a new explosive.

Preparation

The first synthesis was described by Wilhelm Will in 1914, using the reaction between the potassium salt of tetranitroethane with nitric acid.

C<sub>2</sub>(NO<sub>2</sub>)<sub>4</sub>K<sub>2</sub> + 4 HNO<sub>3</sub> → C<sub>2</sub>(NO<sub>2</sub>)<sub>6</sub> + 2 KNO<sub>3</sub> + 2 H<sub>2</sub>O

A practicable method for industrial use starts with furfural, which first undergoes oxidative ring-opening by bromine to mucobromic acid. In the following step, mucobromic acid is reacted with potassium nitrite at just below room temperature to form the dipotassium salt of 2,3,3-trinitropropanal. The final product is obtained by nitration with nitric acid and sulfuric acid at −60 °C.

Properties

The thermal decomposition of hexanitroethane has been detected at 60 °C upwards in both the solid and solution phases. Above 140 °C, this can occur explosively. The decomposition is first order and is significantly faster in solution than in the solid. For the solid, the following reaction can be formulated:

C<sub>2</sub>(NO<sub>2</sub>)<sub>6</sub> → 3 NO<sub>2</sub> + NO + N<sub>2</sub>O + 2 CO<sub>2</sub>

For the decomposition in solution, tetranitroethylene is first formed and can be trapped and detected as a Diels–Alder adduct, for example with anthracene or cyclopentadiene.

References

Further reading

External links