my-server
← Wiki

Hexachlorodisilane

Hexachlorodisilane is the inorganic compound with the chemical formula Si<sub>2</sub>Cl<sub>6</sub>. It is a colourless liquid that fumes in moist air. It has specialty applications in as a reagent and as a volatile precursor to silicon metal.

Structure and synthesis

The molecule adopts a structure like ethane, with a single Si-Si bond length of 233&nbsp;pm.

Hexachlorodisilane is produced in the chlorination of silicides such as e.g. calcium silicide. Idealized syntheses are as follows:

CaSi<sub>2</sub> + 4 Cl<sub>2</sub> → Si<sub>2</sub>Cl<sub>6</sub> + CaCl<sub>2</sub>

Reactions and uses

Hexachlorodisilane is stable under air or nitrogen at temperatures of at least up to 400°C for several hours, but decomposes to dodecachloroneopentasilane and silicon tetrachloride in presence of Lewis bases even at room temperature.

4 Si<sub>2</sub>Cl<sub>6</sub> → 3 SiCl<sub>4</sub> + Si<sub>5</sub>Cl<sub>12</sub>

This conversion is useful in making silicon-based components of use in semiconducting devices including photovoltaic cells.

The compound is also useful reagent for the deoxygenation reactions, such as this general process involving a phosphine oxide:

2 Si<sub>2</sub>Cl<sub>6</sub> + OPR<sub>3</sub> → OSi<sub>2</sub>Cl<sub>6</sub> + PR<sub>3</sub>

References