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Yttrium(III) chloride

Yttrium(III) chloride is an inorganic compound of yttrium and chloride. It exists in two forms, the hydrate (YCl<sub>3</sub>(H<sub>2</sub>O)<sub>6</sub>) and an anhydrous form (YCl<sub>3</sub>). Both are colourless salts that are highly soluble in water and deliquescent.

Structure

Solid YCl<sub>3</sub> adopts a cubic structure with close-packed chloride ions and yttrium ions filling one third of the octahedral holes and the resulting YCl<sub>6</sub> octahedra sharing three edges with adjacent octahedra, giving it a layered structure. This structure is shared by a range of compounds, notably AlCl<sub>3</sub>.

Preparation and reactions

YCl<sub>3</sub> is often prepared by the "ammonium chloride route," starting from either Y<sub>2</sub>O<sub>3</sub> or hydrated chloride or oxychloride. or YCl<sub>3</sub>·6H<sub>2</sub>O. These methods produce (NH<sub>4</sub>)<sub>2</sub>[YCl<sub>5</sub>]:

10 NH<sub>4</sub>Cl + Y<sub>2</sub>O<sub>3</sub> → 2 (NH<sub>4</sub>)<sub>2</sub>[YCl<sub>5</sub>] + 6 NH<sub>3</sub> + 3 H<sub>2</sub>O
YCl<sub>3</sub>·6H<sub>2</sub>O + 2 NH<sub>4</sub>Cl → (NH<sub>4</sub>)<sub>2</sub>[YCl<sub>5</sub>] + 6 H<sub>2</sub>O

The pentachloride decomposes thermally according to the following equation:

(NH<sub>4</sub>)<sub>2</sub>[YCl<sub>5</sub>] → 2 NH<sub>4</sub>Cl + YCl<sub>3</sub>

The thermolysis reaction proceeds via the intermediacy of (NH<sub>4</sub>)[Y<sub>2</sub>Cl<sub>7</sub>].

Treating Y<sub>2</sub>O<sub>3</sub> with aqueous HCl produces the hydrated chloride (YCl<sub>3</sub>·6H<sub>2</sub>O). When heated, this salt yields yttrium oxychloride rather than reverting to the anhydrous form.

Applications

Yttrium chloride is used to make nanocrystals doped with erbium (Er<sup>3+</sup>) and ytterbium (Yb<sup>3+</sup>), such as NaYF<sub>4</sub>:Yb<sup>3+</sup>/Er<sup>3+</sup>.

In electronics and optics, YCl<sub>3</sub> is added to semiconductors, LED materials, and lasers to enhance their performance and stability.

References