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Tungsten borides

Tungsten borides are compounds of tungsten and boron. Their most remarkable property is high hardness. The Vickers hardness of WB or WB<sub>2</sub> crystals is ~20 GPa and that of WB<sub>4</sub> is ~30 GPa for loads exceeding 3 N.

Synthesis

Single crystals of WB<sub>2−x</sub>, x = 0.07–0.17 (about 1&nbsp;cm diameter, 6&nbsp;cm length) were produced by the floating zone method, and WB<sub>4</sub> crystals can be grown by arc-melting a mixture of elemental tungsten and boron.

Structure

WB<sub>2</sub> has the same hexagonal structure as most diborides (AlB<sub>2</sub>, MgB<sub>2</sub>, etc.). WB has several forms, α (tetragonal), β (orthorhombic) and δ (tetragonal).

Properties

δ-WB and WB<sub>2</sub> crystals have metallic resistivities of 0.1 and 0.3 mΩ·cm, respectively. The oxidation of W<sub>2</sub>B, WB and WB<sub>2</sub> is significant at temperatures above 600&nbsp;°C. The final oxidation products contain WO<sub>3</sub> and probably amorphous B<sub>2</sub>O<sub>3</sub> or H<sub>3</sub>BO<sub>3</sub>. The melting temperatures of W<sub>2</sub>B, WB and WB<sub>2</sub> are 2670, 2655 and 2365&nbsp;°C, respectively.

References