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Titanium(III) bromide

Titanium(III) bromide is the inorganic compound with the formula TiBr<sub>3</sub>. It is a blue black paramagnetic solid with a reddish reflection. It has few applications, although it is a catalyst for the polymerization of alkenes.

Production and structure

TiBr<sub>3</sub> can be produced by heating the tetrabromide in an atmosphere of hydrogen:

2TiBr<sub>4</sub> + H<sub>2</sub> → 2TiBr<sub>3</sub> + 2HBr

It can also be produced by comproportionation of titanium metal and titanium tetrabromide.

Ti + 3TiBr<sub>4</sub> → 4TiBr<sub>3</sub>

Two polymorphs of TiBr<sub>3</sub> are known, each exhibiting octahedral Ti centers.

Reactions

Heating the tribromide gives titanium(II) bromide together with the volatile tetrabromide:

2 TiBr<sub>3</sub> → TiBr<sub>4</sub> + TiBr<sub>2</sub>

The solid dissolves in donor solvents (L) such as pyridine and nitriles to produce 3:1 adducts:

TiBr<sub>3</sub> + 3 L → TiBr<sub>3</sub>L<sub>3</sub>

References