my-server
← Wiki

Tellurium tetrafluoride

Tellurium tetrafluoride, TeF<sub>4</sub>, is a stable, white, hygroscopic crystalline solid and is one of two fluorides of tellurium. The other binary fluoride is tellurium hexafluoride. The widely reported Te<sub>2</sub>F<sub>10</sub> has been shown to be F<sub>5</sub>TeOTeF<sub>5</sub> (teflic anhydride). There are other tellurium compounds that contain fluorine, but only the two mentioned contain solely tellurium and fluorine. Tellurium difluoride, TeF<sub>2</sub>, and ditellurium difluoride, Te<sub>2</sub>F<sub>2</sub> are not known.

Preparation

Tellurium tetrafluoride can be prepared reacting tellurium dioxide with sulfur tetrafluoride:

TeO<sub>2</sub> + 2SF<sub>4</sub> → TeF<sub>4</sub> + 2SOF<sub>2</sub>

It is also prepared by reacting nitryl fluoride with tellurium or from the elements at 0&nbsp;°C or by reacting selenium tetrafluoride with tellurium dioxide at 80&nbsp;°C.<br> Fluorine in nitrogen can react with TeCl<sub>2</sub> or TeBr<sub>2</sub> to form TeF<sub>4</sub>. PbF<sub>2</sub> will also fluorinate tellurium to TeF<sub>4</sub>.

Reactivity

Tellurium tetrafluoride will react with water or silica and forms tellurium oxides. Copper, silver, gold or nickel will react with tellurium tetrafluoride at 185&nbsp;°C. It does not react with platinum. It is soluble in SbF<sub>5</sub> and will precipitate out the complex TeF<sub>4</sub>SbF<sub>5</sub>.

Properties

Tellurium tetrafluoride melts at 130&nbsp;°C and decomposes to tellurium hexafluoride at 194&nbsp;°C. In the solid phase, it consists of infinite chains of TeF<sub>3</sub>F<sub>2/2</sub> in an octahedral geometry. A lone pair of electrons occupies the sixth position.

References

General references

  • R.B. King; Inorganic Chemistry of Main Group Elements, VCH Publishers, New York, 1995.
  • W.C. Cooper; Tellurium, VanNostrand Reinhold Company, New York, 1971.