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Rhenium hexafluoride

Rhenium hexafluoride, also rhenium(VI) fluoride, (ReF<sub>6</sub>) is a compound of rhenium and fluorine and one of the seventeen known binary hexafluorides.

Chemistry

Rhenium hexafluoride is made by combining rhenium heptafluoride with additional rhenium metal at 300&nbsp;°C in a pressure vessel.

6 + Re → 7

The compound is a Lewis acid and strong oxidant, adducting potassium fluoride and oxidizing nitric oxide to nitrosyl:

2KF + →
NO + →

Description

Rhenium hexafluoride is a liquid at room temperature. At 18.5&nbsp;°C, it freezes into a yellow solid. The boiling point is 33.7&nbsp;°C.

The solid structure measured at −140&nbsp;°C is orthorhombic space group Pnma. Lattice parameters are a&nbsp;=&nbsp;9.417&nbsp;ÃÂ, b&nbsp;=&nbsp;8.570&nbsp;Å, and c&nbsp;=&nbsp;4.965&nbsp;Å. There are four formula units (in this case, discrete molecules) per unit cell, giving a density of 4.94&nbsp;g·cm<sup>−3</sup>.

The ReF<sub>6</sub> molecule itself (the form important for the liquid or gas phase) has octahedral molecular geometry, which has point group (O<sub>h</sub>). The Re–F bond length is 1.823&nbsp;Å.

Use

Rhenium hexafluoride is a commercial material used in the electronics industry for depositing films of rhenium.

References

Further reading

External links