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Phenylsilver

Phenylsilver is an organosilver compound with the chemical formula . It is a white solid. The structure is a one-dimensional coordination polymer of silver(I) tetrads.

Synthesis

Phenylsilver can be produced by treating silver nitrate with trialkylphenyltin (or trialkylphenyllead at −10 Ã‚°C). In the presence of excess silver nitrate, the reaction produces the bright yellow complex . Phenylsilver can also be produced by treating silver nitrate with diphenylzinc in a 1:2 molar ratio and 0 Ã‚°C. If the molar ratio is 1:1, it will produce orange . Earlier syntheses using phenyl magnesium bromide will produce phenylsilver that contains silver or magnesium salt impurities, which destabilize it.

When heating phenylsilver at a speed of 5 Ã‚°C/min, it decomposes at 67 Ã‚°C. If the heating speed is 10 Ã‚°C/min, it will explode at 47 Ã‚°C.

References

Further reading

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