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Diphenylmethane

Diphenylmethane is an organic compound with the formula (often abbreviated ). The compound consists of methane wherein two hydrogen atoms are replaced by two phenyl groups. It is a white solid.

Diphenylmethane is a common skeleton in organic chemistry. The diphenylmethyl group is also known as benzhydryl.

Synthesis

It is prepared by the Friedel–Crafts alkylation of benzyl chloride with benzene in the presence of a Lewis acid such as aluminium chloride:

Reactivity of the C-H bond

The methylene group in diphenylmethane is mildly acidic with a pK of 32.2, and so can be deprotonated with sodium amide.

The resulting carbanion can be alkylated. For example, treatment with n-bromobutane produces 1,1-diphenylpentane in 92% yield.

Alkylation of various benzhydryl compounds has been demonstrated using the corresponding alkyl halides, both primary (benzyl chloride, β-phenylethyl chloride, and n-octyl bromide) and secondary (benzhydryl chloride, α-phenylethyl chloride, and isopropyl chloride), in yields between 86 and 99%.

The acidity of the methylene group in diphenylmethane is due to the weakness of the , which has a bond dissociation energy (BDE) of . This is well below the published bond dissociation energies for comparable bonds in propane, where the BDE of is , and toluene, where the BDE of is .

See also

References