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Cerium diiodide

Cerium diiodide is an iodide of cerium, with the chemical formula of CeI<sub>2</sub>.

Preparation

Cerium diiodide can be obtained from the reduction of cerium(III) iodide with metallic cerium under vacuum at 800&nbsp;°C to 900&nbsp;°C.

It can also be formed from the reaction of cerium and ammonium iodide in liquid ammonia at −78&nbsp;°C. The reaction forms an ammonia complex of cerium diiodide, which decomposes to cerium diiodide under vacuum at 200&nbsp;°C.

It was first created by John D. Corbett in 1961.

Properties

Cerium diiodide is an opaque dark solid with a metal-like appearance and properties. There is no cerium(II) in cerium diiodide, and its real structure is Ce<sup>3+</sup>(I<sup>−</sup>)<sub>2</sub>e<sup>−</sup>. It is easily hydrolyzed to form the corresponding oxyiodide. Like lanthanum diiodide and praseodymium diiodide, the cerium diiodide forms in the MoSi<sub>2</sub>-type structure, with space group I4/mmm (No. 139).

References