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1,2-Bis(dichlorophosphino)ethane

1,2-Bis(dichlorophosphino)ethane is an organophosphorus compound with the formula (CH<sub>2</sub>PCl<sub>2</sub>)<sub>2</sub>. This colorless liquid is a precursor to chelating diphosphines.

Synthesis and reactions

It is prepared by the reaction of ethylene, white phosphorus, and phosphorus trichloride:

3 C<sub>2</sub>H<sub>4</sub> + 0.5 P<sub>4</sub> + 4 PCl<sub>3</sub> → 3 (CH<sub>2</sub>PCl<sub>2</sub>)<sub>2</sub>

The compound reacts with Grignard reagents and secondary amines to give chelating ligands. An often practiced use of this compound is the synthesis of 1,2-bis(dimethylphosphino)ethane.

Related compounds

References