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(Cyclopentadienyl)titanium trichloride

(Cyclopentadienyl)titanium trichloride is an organotitanium compound with the formula (CH)TiCl. It is a moisture sensitive orange solid. The compound adopts a piano stool geometry.

Preparation and reactions

is prepared by the reaction of titanocene dichloride and titanium tetrachloride:

The complex is electrophilic, readily forming alkoxide complexes upon treatment with alcohols.

Reduction of (cyclopentadienyl)titanium trichloride with zinc powder gives the polymeric Ti(III) derivative (cyclopentadienyl)titanium dichloride:

A related reduction can be effected with cobaltocene:

Other evidence for the Lewis acidity of the trichloride is the ready formation of adducts with phosphine ligands:

See also

References